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NEW ANALYTICAL METHODS & VALIDATION OF EPALRESTAT-BULK & DOSAGE FORMS. EPALRESTAT - ESTIMATION BY USING ULTRA-PERFORMANCE LIQUID CHROMATOGRAPHY & ULTRAVIOLET - VISIBLE SPECTROSCOPY METHODS
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Местонахождение: Алматы | Состояние экземпляра: новый |
Бумажная
версия
версия
Автор: Sharath Chandra Seelam,Kavati Rama Krishna and Kappala Soujanya
ISBN: 9786200586865
Год издания: 2020
Формат книги: 60×90/16 (145×215 мм)
Количество страниц: 148
Издательство: LAP LAMBERT Academic Publishing
Цена: 36982 тг
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Аннотация: Epalrestat is an anti-diabetic drug. It is not official in any pharmacopoeia. Literature survey reveals that only two RP-HPLC methods were developed for Epalrestat but no methods were reported in UPLC and Derivative Spectroscopy for determination of Epalrestat. In the present investigation, we have developed a UV spectrophotometric and UPLC methods for the quantitative estimation of Epalrestat in bulk drug and tablet formulations. The UPLC method is promising with more sensitive accurate and precise compared to the UV spectrophotometric methods. The results obtained with proposed methods confirm the suitability of these methods for tablet dosage forms. The other active ingredients and excipients usually present in the tablet dosage forms did not interfere in the estimation, where some commercial dosage forms were analyses by these methods. The accuracy of the methods was confirmed by the recovery studies. The methods can be used for the routine determination of Epalrestat in bulk and in tablet dosage forms.
Ключевые слова: Epalrestat, Ultra performance liquid chromatography, ULTRA VIOLET - VISIBLE SPECTROSCOPY, DERRIVATIVE SPECTROSCOPY, High Performance Liquid Chromatography, pharmaceutical analysis, UPLC, HPLC, UV Spectroscopy, Diabetes mellitus, SEPERATION TECHNIQUES
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